By Edward R Dougherty
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Because of the relatively high doses used, they should have good water solubility. They should be nontoxic at the dose required to give the required imaging effect; 1/T1 changes as small as 10 to 20% can be detected by MRI. T1 agents are typically gadolinium(III) complexes, manganese(II) complexes, or, in several animal studies, just the Mn2+ cation3,4 (given as MnCl2; see also Chapter 20 for another Mn2+ application). S. and Europe. fm Page 17 Friday, February 9, 2007 5:16 AM Physicochemical Principles of MR Contrast Agents 17 Chemically, the gadolinium (Gd) compounds exhibit similar features: an eight-coordinate ligand binding to Gd and a single water molecule coordinated to Gd.
This relaxation and fast water exchange catalytically enhances the relaxation rate of the bulk water. In addition, water not contained in the ﬁrst coordination sphere can also be relaxed by the ion. This water is classiﬁed into two groups: second-sphere water, which denotes water molecules that directly hydrate the complex and have a lifetime in the second sphere longer than the time constant for water diffusion, and outersphere water, which is not associated with the complex but is diffusing nearby.
Can be increased by going to higher ﬁelds since chemical shift in frequency units (hertz or radians/second) is directly proportional to applied ﬁeld. 54 Other paramagnetic lanthanides, but not gadolinium, are capable of inducing large chemical shifts. 11) that contain two sources of exchangeable hydrogen — the coordinated water and the amide N-H. With the DOTAM ligand, water exchange is so slow that the gadolinium analog is not useful as a T1 agent. However, the slow water exchange does mean that the Δωτ > 1 requirement is met.