By Joseph Sherma (Eds.)
ISBN-10: 0127843167
ISBN-13: 9780127843162
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Prepare a standard reference curve by injecting several known concentrations of fenoxycarb (2-200 ng). Determine background by processing an untreated sample from the same origin as the sample. Determine recovery by spiking untreated samples and processing them as described above. vi. Calculation. Determine the amount of fenoxycarb in a sample expressed as micrograms per gram by measuring peak area and comparing with the standard reference curve. Calculate the ppm-value as follows: ppm ^g/g) fenoxycarb = p „_ where A = fenoxycarb in the injected volume as determined from the standard reference curve (ng) B = volume of sample injection (μΐ) C = volume of mobile phase in sample (ml) D = weight of commodity equivalent in sample solution (g) R = rate of recovery (%) e.
Residue Analysis 1. PRINCIPLE Chlorimuron ethyl is extracted from soybeans in méthylène chloride or ethyl acetate and from wheat grain, corn kernels, turnips, and potatoes in ethyl acetate. The soybean extracts can be cleaned up by either solvent partitioning followed by silica solid-phase extraction or by medium-pressure liquid chromatography on a silica column. The wheat grain and corn kernel extracts are cleaned up by the medium-pressure liquid chromatography. Turnip and potato extracts can be cleaned up by solvent partitioning followed by silica solid-phase extraction (potatoes) or hydrophobic (C18) solid-phase extraction (potatoes).
Use a 20-μ1 loop for sample processing procedure 1 (Section II,B,4,b) and a 10-μ1 loop for sample processing procedures 2 and 3 (Sections II,B,4,C and II,B,4,d). 6. 10 ppm) with the analysis of each set of samples. Use the minimum quantifiable amount of chlorimuron ethyl standard in either méthylène chloride (sample processing procedure 1) or ethyl acetate (sample processing procedures 2 and 3) for fortifications and preparation of standards. Pipet proper amounts for standards into test tubes and remove the solvent under a stream of nitrogen.