By Georges Guiochon
ISBN-10: 352732898X
ISBN-13: 9783527328987
ISBN-10: 352764928X
ISBN-13: 9783527649280
Thoroughly revised to mirror the advancements during this fast-changing box, this new version gains 35 % new content material. It keeps the interdisciplinary strategy that elegantly combines the chemistry and engineering concerned to explain the perception and development of chromatographic approaches. It additionally covers fresh advances in preparative chromatographic procedures for the separation of "smaller" molecules utilizing common laboratory gear in addition to the targeted belief of business chemical crops. the rise in biopharmaceutical ingredients is mirrored by way of new and revised chapters on assorted alterations of constant chromatography in addition to ion-exchange chromatography and different separation rules common in biochromatography.
Following an introductory part at the historical past of chromatography, the present country of study and the layout of chromatographic strategies, the e-book is going directly to outline the overall terminology. There then persist with sections on desk bound stages, choice of chromatographic platforms and approach recommendations. a very new bankruptcy bargains with engineering and operation of chromatographic apparatus. ultimate chapters on modeling and backbone of version parameters in addition to version established layout, optimization and keep watch over of preparative chromatographic tactics permit for optimum collection of chromatographic processes.
crucial for chemists and chemical engineers within the chemical, pharmaceutical, and nutrients industries.
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Extra resources for Preparative Chromatography, Second Edition
Sample text
Other passages are devoted to plate numbers, HETP values as well as their determination based on first and second moments. The experienced reader may pass quickly through this chapter to become familiar with definitions used. For beginners this chapter is recommended in order to learn the general terminology and acquire a basic understanding. A further goal of this chapter is the harmonization of general chromatographic terms between engineers and chemists. Chapter 3 focuses on stationary phases and the selection of chromatographic systems.
In case of isocratic and gradient SMB processes, rigorous process simulations combined with short-cut calculations based on the TMB-model are useful tools for process optimization, which is illustrated by different example cases. Further sections discuss the improvements of SMB chromatography by variable operating conditions as given by Varicol, PowerFeed, or ModiCon processes. Finally, the latest scientific results on model-based advanced control of SMB processes are presented which are thought to be of increasing importance for practical applications.
Seidel-Morgenstern. # 2012 Wiley-VCH Verlag GmbH & Co. KGaA. Published 2012 by Wiley-VCH Verlag GmbH & Co. KGaA. 8 j 2 Fundamentals and General Terminology Regarding chromatographic separation, the homogeneous mixture phase is a fluid. The additional second phase is a solid or a second immiscible fluid. The driving force for transport between the phases is the deviation of the compositions from the equilibrium state. The mixture introduced is separated by selective relative movements of the components between the two phases.